Quantitative determination of carbon in organic compounds

VC2.1.1.1
Quantitative determination of carbon in organic compounds
Quantitative determination of carbon in organic compounds

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Description

In experiment C2.1.1.1, the carbon content of an organic compound is determined quantitatively. In a combustion analysis, the substance is passed over glowing copper(II) oxide at approx. 800 °C - 900 °C. The carbon is converted to CO2 and the hydrogen is converted to H2O. The CO2 gas generated is collected in a gas syringe and the volume is measured.

Components of equipment sets

1 664069 Reaction tube, quartz, 220 x 25 mm Ø, for butane combustion LD
2 665374 Drying tube, 1 GL 18 and 1 GL 25, 120 mm x 30 mm diam. LD
2 665914  4  Gas syringe, 100 ml with 3-way stopcock LD
1 656017  4  Teclu burner, universal LD
1 666724  8  Wide-flame attachment LD
1 666729  4  Safety gas hose, 1 m LD
1 666603  4  Base rail, 95 cm LD
4 666609  4  Stand tube, 45 cm, Ø 10 mm LD
4 666615  4  Universal bosshead LD
5 30109  4  Bosshead S LD
4 666555  4  Universal clamp 0...80 mm LD
1 30172  4  Universal clamp, 0...120 mm LD
1 666962  4  Spatula, double ended, 150 mm LD
1 665994  4  Graduated pipette 1 ml LD
1 666003  4  Pipetting ball (Peleus ball) LD
1 667180  4  Rubber tubing 7 mm Ø, 1 m LD
1 604481  4  Rubber tubing, 1 m x 4 mm diam., DIN 12865 LD
1 665004  4  Funnel, Boro 3.3, 80 mm diam. LD
1 604510  4  Tubing connector, 4...15 mm LD
1 661000  4  Minican pressurised gas canister, nitrogen LD
GHS04 Warning H280
1 660989  4  Minican pressurised gas canister, n-Butane LD
GHS02GHS04 Danger H220 H280
1 660980  4  Fine regulating valve for minican gas canisters LD
1 667034  4  Tweezers, blunt, 200 mm LD
1 6729410  4  Copper(II) oxide, wire form, 250 g LD
GHS07GHS09 H302 H410
1 6712410  4  Calcium chloride, granulated, 250 g LD
GHS07 H319
1 6744310  4  1-Propanol, 250 ml LD
GHS02GHS05GHS07 H225 H318 H336
1 6721010  4  Glass wool, 100 g LD

Experiment Instructions

PDF (Experiment description) PDF (Experiment description) C2.1.1.1 Quantitative determination of carbon
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