Determination of the melting point of salicylic acid

VC3.1.3.1
Determination of the melting point of salicylic acid
Determination of the melting point of salicylic acid

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Description

In experiment C3.1.3.1, the thiele tube is used to determine the melting point of salicylic acid. The melting point is, along with the boiling point, a characteristic property of every substance. The melting point determination apparatus is filled with paraffin and fitted with a thermometer. A melting point tube is filled with the substance to be assayed. The tube is inserted with the open side into the device in a way that it is positioned alongside the thermometer. The melting point is determined by slow heating in the water bath.

Components of equipment sets

1 667500 Melting point determination apparatus LD
1 661085  4  Melting point detection tubes, set of 100 LD
1 667306  4  Silicone gaskets, GL 18/6, set of 10 LD
1 666161  4  Chemical thermometer, -10...+250 °C/1 K LD
1 6668471  8  Magnetic stirrer with hotplate LD
1 666854  4  Stirring magnet, 50 mm x 8 mm diam. LD
1 666523  4  Stand rod, 450 x 12 mm diam., M10 thread LD
1 666555  4  Universal clamp 0...80 mm LD
1 30109  4  Bosshead S LD
1 602725  4  Laboratory dish, 140 mm diam., 900 ml LD
1 664154  4  Watch glass dish 80 mm Ø LD
1 6045682  4  Powder spatula, steel, 185 mm LD
1 665009  4  Funnel PP 75 mm Ø LD
1 656017  4  Teclu burner, universal LD
1 667187  4  Safety gas hose, 1 m LD
1 6740820  4  Paraffin, thick, 1 l LD
1 6746210  4  Salicylic acid, 100 g LD
GHS05GHS07 H302 H318

Experiment Instructions

PDF (Experiment description) PDF (Experiment description) C3.1.3.1 Determination of the melting point of salicylic acid
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